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weighing 4.2 g (14mmol) of Fmoc-Gly-OH, 2.2 g (16.8mmol) of HOBt and 0.2 g (1.4mmol) of DMAP, dissolving with DMF, adding 3.0ml of DIC (20mmol) in ice-water bath at 0 , activating for 5 minutes, adding into a reaction column, reacting for 2 hours, adding 35ml of acetic anhydride and 30ml of pyridine, mixing and sealing for 24 hours, washing three times with DCM, draining the Resin after methanol contraction to obtain 21.8 g of 1- (3-hydroxypropyl) -1H-imidazole trifluoromethanesulfonic acid-Merrifield Resin in total, wherein the detection substitution degree is 0.30 mmol/g

to as late as the early evening

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Quast, D., Schenker, N., Menge, B., Nauck, M., Kapitza, C., Meier, J